2017-Sustainable Industrial Processing Summit
SIPS 2017 Volume 5. Marquis Intl. Symp. / New and Advanced Materials and Technologies

Editors:Kongoli F, Marquis F, Chikhradze N
Publisher:Flogen Star OUTREACH
Publication Year:2017
Pages:590 pages
ISBN:978-1-987820-69-0
ISSN:2291-1227 (Metals and Materials Processing in a Clean Environment Series)
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    The Properties and Microstructure Evolution of Cast Austenite Stainless Steel under Thermal Aging

    Fei Xue1; Xiao Jin1; XiangBing Liu1; Xitao Wang2;
    1SUZHOU NUCLEAR POWER RESEARCH INSTITUTE, Suzhou, China; 2UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING, Beijing, China;
    Type of Paper: Invited
    Id Paper: 142
    Topic: 43

    Abstract:

    In this paper, cast austenite duplex stainless steel from main circulating pipe are aged at 400°C for different times, the properties are studied during aging, and the mechanism of material is investigated by microstructure evolution characterization at same aging time. The results show the tensile strength increased nearly 12%, reduction of area decreased nearly 21%, and impact ductility decreased nearly 50%. The reason lies in the ferrite phase becoming weak and harmful to mechanical properties after aging. Transmission electron microscope (TEM) and three dimensional atom probe (3DAP) are used to study the microstructure evolution during aging, effect of aging on duplex stainless steel by spinodal decomposition in ferrite phase, Cr-rich phase formed from Cr-rich segregated region by the concentration of Cr atoms in it after being aged 3000h, and the size of Cr-rich phase between 5-10nm, and then, the difficulty of increased slipping in dislocation and aggregated dislocations, resulting in the local stress concentration around the Cr-rich phase. The phenomenon of spinodal decomposition is that as the aging time and content of Cr in Cr-rich cluster increases, the more stress is required during the deformation, which causes higher level of stress triaxiality ratio; with this focus, dislocations get across the Cr-rich phase, which disperses in ferrite phase and slipping, the plastic deformation is more easily reached, and leads to the decreased of ductility.

    Keywords:

    Materials; Measurement; Steel;

    References:

    [1] K Seiichi, S Naruo, T Genta and Al Et. Microstructural changes and fracture behavior of CF8M duplex stainless steels after long term aging. Nuclear Engineering and Design, 174 (1997), 273-285.
    [2] M Hyde J., K Miller M., A Cerezo and Al Et. A study of the effect of ageing temperature on phase separation in Fe45%Cr alloys. Applied Surface Science, 87-88 (1995), 311-317.
    [3] T Yamada, S Okano and H Kuwano. Mechanical property and microstructural change by thermal aging of SCS14A cast duplex stainless steel. Journal of Nuclear Materials, 350 (2006), 47-55.
    [4] J Vojvodič-Tuma, B Šuštaršič and F Vodopivec. The effect of ageing temperature and time on the mechanical properties of FeNiCrMo alloys with different contents of ferrite. Nuclear Engineering and Design, 238 (2008), 1511-1517.
    [5] M Nystrom and B Karlsson. Fatigue of duplex stainless steel influence of discontinuous, spinodally decomposed ferrite. Materials Science and Engineering. A, 215 (1996), 26-38.
    [6] K Chopra O. Estimation of fracture toughness of cast stainless steels during thermal aging in LWR Systems, in Book Estimation of fracture toughness of cast stainless steels during thermal aging in LWR Systems. Argonne National Laboratory, 1994.
    [7] F Iacoviello, F Casari and S Gialanella. Effect of 475 C embrittlement on duplex stainless steels localized corrosion resistance. Corrosion Science, 47 (2005), 909-922.
    [8] W Zhang, L Jiang, J Hu and Al Et. Effect of ageing on precipitation and impact energy of 2101 economical duplex stainless steel. Materials Characterization, 60 (2009), 50-55.
    [9] Mats Hättestrand, Petter Larsson, Guocai Chai and Al Et. Study of decomposition of ferrite in a duplex stainless steel cold worked and aged at 450–500°C. Materials Science and Engineering A, 499 (2009), 489-492.
    [10] J Wang, H Zou, C Li and Al Et. The effect of microstructural evolution on hardening behavior of type 174PH stainless steel in long term aging at 350 °C. Materials Characterization, 57 (2006), 274-280.
    [11] S Kawaguchi, N Sakamoto, G Takano and Al. Et. Microstructural changes and fracture behavior of CF8M duplex stainless steels after long term aging. Nuclear Engineering and Design, 173 (1997), 273-285.
    [12] Xue Fei, Wang Zhao-Xi, Zhang Guo-Dong, Qu Bao-Ping, Shi Hui-Ji, Shu Guo-Gang and Liu Wei. SCI-Numerical simulations of the phase separation properties for the thermal aged CDSS with Phase Field Model. Nuclear Engineering and Design, 241 (2011), 2378-2385.
    [13] A Hishinuma, A Kohyama, L Klueh R. and Al. Et. Current status and future R&D for reduced-activation ferritic/martensitic steels. Journal of Nuclear Materials, 258-263 (1998), 193-204.
    [14] H Kim S., S Byun T., S Lee B. and Al. Et High Temperature Deformation Behavior and Flow Softening Mechanism of TiAl Intermetallic Compound., in Book High Temperature Deformation Behavior and Flow Softening Mechanism of TiAl Intermetallic Compound. Chang-won, South Korea, 1998: 156-160.

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    Cite this article as:

    Xue F, Jin X, Liu X, Wang X. (2017). The Properties and Microstructure Evolution of Cast Austenite Stainless Steel under Thermal Aging. In Kongoli F, Marquis F, Chikhradze N (Eds.), Sustainable Industrial Processing Summit SIPS 2017 Volume 5. Marquis Intl. Symp. / New and Advanced Materials and Technologies (pp. 146-156). Montreal, Canada: FLOGEN Star Outreach