2017-Sustainable Industrial Processing Summit
SIPS 2017 Volume 8: Surfaces and Interfaces(SISAM), Composite, Ceramic and Nanomaterials

Editors:Kongoli F, Braems I, Demange V, Dubois JM, Pech-Canul M, Patino CL, Fumio O
Publisher:Flogen Star OUTREACH
Publication Year:2017
Pages:249 pages
ISBN:978-1-987820-75-1
ISSN:2291-1227 (Metals and Materials Processing in a Clean Environment Series)
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    Synthesis and Characterization of Zeolite Membranes on Zirconia and Calcium Silicate Substrates

    Adriana Medina Ramirez1; Gabriela Maricela Gonzalez Vega2; Georgina Garcia3; Beatriz Ruiz Camacho4;
    1UNIVERSIDAD DE GUANAJUATO, CAMPUS GUANAJUATO, Guanajuato, Mexico; 2UNIVERSITY OF LA CIENEGA, sahuayo de morelos, Mexico; 3UNIVERSITY OF LA CIENEGA, Sahuayo, Mexico; 4UNIVERSIDAD DE GUANAJUATO, Guanajuato, Mexico;
    Type of Paper: Regular
    Id Paper: 75
    Topic: 18

    Abstract:

    In the present work we report the synthesis of zeolite membrane on zirconium oxide and calcium silicate supports by secondary growth method. The effect of type of zeolite was evaluated on the formation of a homogeneous zeolite layer. Zirconia and calcium silicate disks of one centimeter of diameter were functionalized by (3-Mercaptopropyl)trimethoxysilane (MPS) and then they were rubbed with zeolite seeds. Two zeolite types were studied: LTA and MER. The functionalized substrates were submitted to hydrothermal treatment at 100°C, for 4 h and 175°C for 16h for LTA and MER zeolites, respectively. The products were characterized by SEM, XRD and IR techniques. The results indicated that the LTA zeolite led to formation of a homogeneous zeolite membrane on both substrates. While MER zeolite membrane only was obtained on the zirconia substrate. The nature of the substrate and the MPS had an important effect on the zeolite type growth on the substrate. The homogeneous zeolite membranes were soaked in a simulated body fluid in order to evaluate the formation of apatite layer this response could be associated to possible applications as bone filler.

    Keywords:

    Ceramic; Crystallization; Materials; Synthesis;

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    Cite this article as:

    Medina Ramirez A, Gonzalez Vega G, Garcia G, Ruiz Camacho B. (2017). Synthesis and Characterization of Zeolite Membranes on Zirconia and Calcium Silicate Substrates. In Kongoli F, Braems I, Demange V, Dubois JM, Pech-Canul M, Patino CL, Fumio O (Eds.), Sustainable Industrial Processing Summit SIPS 2017 Volume 8: Surfaces and Interfaces(SISAM), Composite, Ceramic and Nanomaterials (pp. 196-203). Montreal, Canada: FLOGEN Star Outreach