2025 - Sustainable Industrial Processing Summit
SIPS2025 Volume 10. Intl. Symp on Energy, Carbon, Battery, Biochar and Agroforestry

Editors:F. Kongoli, S.M. Atnaw, H. Dodds, T. Turna, J. Antrekowitsch, G. Hanke, K. Aifantis, Z. Bakenov, C. Capiglia, V. Kumar, A.U.H. Qurashi, A. Tressaud, R. Yazami, M. Giorcelli
Publisher:Flogen Star OUTREACH
Publication Year:2025
Pages:316 pages
ISBN:978-1-998384-56-3 (CD)
ISSN:2291-1227 (Metals and Materials Processing in a Clean Environment Series)
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    MULTIMODAL CHARACTERIZATION AND APPLICATION POTENTIAL OF CARBON FROM METHANE PYROLYSIS IN METALLIC MELTS

    Philip Aster1; Juergen Antrekowitsch2;
    1TECHNICAL UNIVERSITY OF LEOBEN, Leoben, Austria; 2CHAIR OF NONFERROUS METALLURGY, UNIVERSITY OF LEOBEN, Leoben, Austria;
    Type of Paper: Invited
    Id Paper: 127
    Topic: 39

    Abstract:

    Carbon produced via methane pyrolysis in metallic melts represents a promising sustainable alternative to conventional graphite. This material combines a CO₂-reduced production pathway with physical and chemical properties that can be tailored for high-performance applications. Due to the presence of metallic residues (e.g., Cu, Fe, Sn) introduced during the pyrolysis process, a comprehensive analytical approach is required to evaluate its structural integrity, purity, and functionality [1].

    This study presents a multimodal characterization strategy combining Raman spectroscopy, scanning electron microscopy (SEM), and X-ray fluorescence analysis (XRF). Raman spectroscopy provides detailed insights into carbon bonding states, crystallinity, and defect density, particularly through the evaluation of D-, G-, and 2D-bands. SEM imaging enables morphological analysis, surface topology assessment, and particle size evaluation at sub-micrometer resolution. XRF complements these methods by quantifying trace metallic impurities originating from the melt environment, which may influence subsequent material processing and application behavior [2,3].

    The obtained results serve as a basis for targeted purification and refinement processes that enable the use of pyrolysis-derived carbon as a functional material across a wide range of applications. Potential use cases include bipolar plates for fuel cells, anode materials for lithium-ion batteries, electrically conductive polymers, expandable flame-retardant fillers, lubricants, and electrodes for electric arc furnaces. The unique combination of graphite-like properties with a sustainable synthesis route addresses the increasing industrial demand for environmentally friendly high-performance materials. A central challenge remains the precise adjustment of material characteristics to meet specific performance requirements in each application sector [4–6].

    Keywords:

    Methane pyrolysis; Sustainable Graphite Replacement; Carbon materials; Industrial applications

    Cite this article as:

    Aster P and Antrekowitsch J. (2024). MULTIMODAL CHARACTERIZATION AND APPLICATION POTENTIAL OF CARBON FROM METHANE PYROLYSIS IN METALLIC MELTS. In F. Kongoli, S.M. Atnaw, H. Dodds, T. Turna, J. Antrekowitsch, G. Hanke, K. Aifantis, Z. Bakenov, C. Capiglia, V. Kumar, A.U.H. Qurashi, A. Tressaud, R. Yazami, M. Giorcelli (Eds.), Sustainable Industrial Processing Summit Volume 10 Intl. Symp on Energy, Carbon, Battery, Biochar and Agroforestry (pp. 273-274). Montreal, Canada: FLOGEN Star Outreach